Synthesis and characterization of (3-aminopropyl) triethoxysilane (APTES) functionalized zeolite AlPO-18
學年 110
學期 1
出版（發表）日期 2021-11-01
作品名稱 Synthesis and characterization of (3-aminopropyl) triethoxysilane (APTES) functionalized zeolite AlPO-18
作品名稱（其他語言）
著者 L.D. Anbealagan; T.L. Chew; Y.F. Yeong; Z.A. Jawad; Chii-Dong Ho
單位
出版者
著錄名稱、卷期、頁數 IOP Conference Series: Materials Science and Engineering 1195, 012047
摘要 Over the years, functionalization of zeolite is gaining popularity among researchers to further modify the properties of the zeolite for wide applications. The procedure of functionalization is crucial to ensure that the framework and structure of the zeolite would not be destroyed by the functionalization process. In this work, zeolite AlPO-18 was synthesized via hydrothermal synthesis method and functionalized by (3-Aminopropyl) triethoxysilane (APTES). The effect of the APTES functionalization on zeolite AlPO-18 was investigated in this work. Both unfunctionalized and silane-functionalized zeolite AlPO-18 were characterized using Fourier-transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), and Thermogravimetric analysis (TGA) for their properties. The morphology and the composition of the elements present in zeolite AlPO-18 and zeolite NH2-AlPO-18 were examined using Field Emission Scanning Electron Microscopy (FESEM) and Energy-Dispersive spectroscopy (EDX) respectively. The XRD pattern of NH2-AlPO-18 was similar to that of zeolite AlPO-18, however, the intensity of the peaks was lower compared to zeolite AlPO-18. Based on the FTIR spectra, the presence of N-H stretching and bending vibration band of aminosilane were observed in the NH2-AlPO-18 sample. According to FESEM images, the morphology of NH2-AlPO-18 was comparable to that of zeolite AlPO-18 even after functionalization, proving that functionalization of aminosilane on zeolite does not affect on the zeolite structure. Besides that, EDX proves the presence of 3.02 % of element N in the NH2-AlPO-18 sample which is absent in the zeolite AlPO-18 sample. All of the characterizations evinced the presence of aminosilane, APTES in the NH2-AlPO-18 sample.
關鍵字
語言 en_US
ISSN 1757-899X
期刊性質 國外
收錄於 EI
產學合作
通訊作者
審稿制度 否
國別 GBR
公開徵稿
出版型式 ,電子版,紙本
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